Dissertation
Dissertation > Industrial Technology > General industrial technology > Materials science and engineering > Special structural materials

Synthesis and Characterization of Sulfide and Its Heterostructures

Author LiuYuFeng
Tutor FangZhen
School Anhui Normal University
Course Inorganic Chemistry
Keywords Solvothermal Characterization Photocatalytic Properties Optoelectronic properties
CLC TB383.1
Type Master's thesis
Year 2011
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The sulfide and heterostructures nanomaterials is important semiconductor material , it has many unique applications , such as photocatalysts , photoelectric materials . This thesis solvothermal method , successfully prepared CdS nano triangle / bismuth sulfide nanowire heterostructures homogeneous Cu1.8S , rattles shaped core-shell structure and AgBiS 2 mace -like nanostructures . The main research work as follows: 1. Cadmium nitrate , anhydrous bismuth chloride , thiourea in the thermal condition of the solvent is synthesized CdS triangle / bismuth sulfide nanowire heterostructure preliminary inquiry amount of thiourea , and the reaction temperature , reactant concentration, the impact on the product . The resulting products were using X-ray diffraction ( XRD ) , field emission scanning electron microscope ( FESEM ) , transmission electron microscopy ( TEM ) , high-resolution transmission electron microscopy ( HRTEM ) , selected area electron diffraction (SAED), photoluminescence (PL ) and the like to characterize . Studies have shown that cadmium sulfide nano triangle / bismuth sulfide nanowire heterostructures has good photocatalytic properties . Copper nitrate , thiourea as raw material , synthesized by solvothermal method a homogeneous Cu1.8S rattles shaped structure ( RTS ) , the resulting product were used SEM , transmission electron microscopy (TEM) , X -ray photoelectron spectroscopy ( XPS ) , infrared spectroscopy (IR) and other characterization. The studies show Cu1.8S RTS has a good photoelectric effect . Silver nitrate , anhydrous bismuth chloride as raw materials in the solvothermal conditions . Prepared AgBiS 2 mace -like nanostructures , the product were used XRD , SEM, TEM characterize . Preliminary study of the conditions such as temperature and concentration , and found that the concentration on the morphology of the product has an important role .

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